1000218-992有機化學實驗進度

 

No.

Date

 

Topic                                                                                                                           

page

1

2/24

 

Check in

 

 

3/3

 

Safety VCR /Break

 

2

3/10

Exp.1

Simple Distillation of Ethanol Compound

 

66

3

3/17

Exp.2

Extraction with Solvents: Separation of Benzoic Acid and Acetanilide

 

117

4

3/24

Exp.3

Chromatography: 1. TLC

Synthesis α-methylbenzyl alcohol from Acetophenone 

 

5

3/31

 

Spring Vacation(停課)

 

 

6

4/7

Exp.4

Chromatography: 2. FC

Improvements in the Separation of β-Carotene and Lycopene by Column Chromatography

 

7

4/14 

Exp.5

Identification of Organic Compounds:

A.     Hydrocarbons: (1)Permanganate Test(Baeyer Test)                

              (2)Bromine Test(demo.)

B.     Alkyl Halides: (1)Alcoholic Silver Nitrate                                       

              (2)Sodium Iodide in Acetone

 

 

177

 

178

 

8

4/21

Exp.6

Functional Group Identification (alcohols):

A.     Ritter Test

B.     Lucas Test

C.     Iodoform Test

 

166

9

4/28

Exp.7

Functional Group Identification (Ald & Ketones):

A. 2,4-Dinitrophenylhydrazone Test

B. Tollen’s Reagent (Silver mirror Test)

C. Schiff’s Fuchsin Test

 

 

187

169

170

 

 

10

5/5

Exp.8

Preparation of Poly Vinyl Alcohol

 

11

5/12

Exp.9

Preparation of Azo Dyes: Methyl Orange 

 

12

5/19

Exp.10

Unknown Sugar Solution Test

 

13

5/26

 

Final Exam & Check out

 

Text Book: Charles F. Wilcox, Jr.

“Experimental Organic Chemistry: A Small-Scale Approach” 2nd edition

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