1030218-102(2)外系有機化學進度

 The Schedule of Organic Chemistry Laboratory

生一乙有機化學實驗 (2nd semester, 2014)

 

No.

Date

 

Topic                                                                                                                          

page

1

2/18

 

Check in :Basic Laboratory Operations

 

 

2/25

 

Break

 

2

3/04

Exp.1

Simple Distillation of Ethanol Compound

(參考講義Chap.5 Simple and Fractional Distillation)

 

66

3

3/11

Exp.2

Extraction with Solvents: Separation of Benzoic Acid and Acetanilide

(參考講義 Chap.9 Extraction with Solvents)

117

4

3/18

Exp.3

Chromatography: 1. TLC

Synthesis α-methylbenzyl alcohol from Acetophenone

(參考講義 Chap.10 Chromatography)

 

5

3/25

Exp.4

Chromatography: 2. FC

Improvements in the Separation of β-Carotene and Lycopene by Column Chromatography(參考講義 Chap.10 Chromatography)

 

6

4/01

 

Spring Vacation(停課)

 

7

4/08

Exp.5

Preparation of Poly Vinyl Alcohol

 

8

4/15

 

Mid-Term Examination(停課)

 

9

4/22

Exp.6

Identification of Organic Compounds:

<![if !supportLists]>A.    <![endif]>Hydrocarbons: (1)Permanganate Test(Baeyer Test)                

            (2)Bromine Test (Demo.)

<![if !supportLists]>B.     <![endif]>Alkyl Halides: (1)Alcoholic Silver Nitrate

(參考講義Chap.11 Identification by Chemical Methods)                                  

             (2)Sodium Iodide in Acetone

 

 

177

 

178

 

10

4/29

Exp.7

Functional Group Identification (alcohols):

<![if !supportLists]>A.    <![endif]>Ritter Test

<![if !supportLists]>B.     <![endif]>Lucas Test

<![if !supportLists]>C.     <![endif]>Iodoform Test

(參考講義Chap. 11 Identification by Chemical Methods)

 

166

11

5/06

Exp.8

Functional Group Identification (Ald & Ketones):

A. 2,4-Dinitrophenylhydrazone Test

B. Tollen’s Reagent (Silver Mirror Test)

C. Schiff’s Fuchsin Test

(參考講義Chap. 11 Identification by Chemical Methods)

 

187

169

170

 

 

12

5/13

Exp.9

Preparation of Azo Dyes: Methyl Orange 


13

5/20

Exp.10

Unknown Sugar Solution Test

 

14

5/27

 

Final Exam & Check out

 

 

Text Book: Charles F. Wilcox, Jr.

“Experimental Organic Chemistry: A Small-Scale Approach” 2nd edition

                                       2014.2

附註:實驗成績評定標準

        出缺席狀況與實驗態度15%

        預習實驗、結果、成品15%

        實驗報告40% (Late 80%Repeat 90%)

        期末考30%

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